Improved sample environment for in situ neutron powder diffraction using sapphire single-crystal cells
The present proposal aims for several improvements concerning the sample alignment in order to optimize beamtime usage, a new heating system for in situ powder diffraction at D20 and a validation of a newly developed gas pressure cell. A x/y/z/omega-stage has been developed and will be tested. Further, a new heating system will be tested in order to reach higher temperature and allowing simultaneous raman spectroscopy and neutron diffraction. Additionally, Six new and untested sapphire single crystals need to be characterized by omega scans on the neutron diffractometer D20 to test their suitability for in situ neutron powder experiments. Finally, the validation of a newly developed gas pressure cell needs to be redone due to technical issues (see experimental report Test 2994).
The data is currently only available to download if you are a member of the proposal team.
The recommended format for citing this dataset in a research publication is in the following format:
FINGER Raphael; GOETZE André; Thomas C. Hansen; KEILHOLZ Simon; Holger Kohlmann and WIDENMEYER Marc. (2020). Improved sample environment for in situ neutron powder diffraction using sapphire single-crystal cells. Institut Laue-Langevin (ILL) doi:10.5291/ILL-DATA.5-24-639
This data is not yet public
This data is not yet public
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