DOI > 10.5291/ILL-DATA.6-06-449

This proposal is publicly available since 02/24/2018

Title

High energy neutron powder diffraction on graphene and metal-decorated graphene

Abstract

Graphene is a very promising material and appears particularly suitable for developing efficient hydrogen storage systems, if it is “decorated” with proper metal ions. Recently, we managed to produce gram-scale bulk defective graphene by chemical methods and to decorate it with Lithium and Nickel atoms. Although a structural characterization of chemically synthesized graphene is missing, the investigation of the defects as well as of the decorating metal local environment is a fundamental prerequisite in order to develop an efficient graphene-based gas storage device. Hence we propose to investigate the morphology of these systems at the nanoscale, by means of high energy neutron diffraction and atomic pair distribution function (PDF) data analysis using the D4 diffractometer at the ILL.

Experimental Report

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Data Citation

The recommended format for citing this dataset in a research publication is in the following format:

CAVALLARI Chiara; ARAMINI Matteo; BRUNELLI Michela; Henry E. Fischer; Mattia Gaboardi; PONTIROLI Daniele; RICCO Mauro; ROLS Stephane and VLACHOPOULOU Georgia. (2013). High energy neutron powder diffraction on graphene and metal-decorated graphene. Institut Laue-Langevin (ILL) doi:10.5291/ILL-DATA.6-06-449

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Metadata

Experiment Parameters

  • Experiment energy

    0.5A
  • Experiment moment

    0.35 - 23.5 A^-1
  • Experiment res energy

    as available
  • Experiment res moment

    as available

Sample Parameters

  • Formula

    • Chemically synthesized graphene(exfoliated graphite oxide) and metal decorated graphene (LiC3 and NiC80)
  • Consistence

    powder
  • Mass

    500