DOI > 10.5291/ILL-DATA.8-01-390

This proposal is publicly available since 11/15/2017

Title

Neutron studies of alpha-chitin

Abstract

Polysaccharides having simple molecular structure such as cellulose, chitin, and amylose represent the major part of biomass and have great potential as renewable resources. Determining their detailed structures and hydrogen bonding arrangements is a key to understanding and improving their properties and utilization. X-rays provide the positions of O and C atoms, whereas neutrons in addition provide the positions of H atoms. We would like to collect neutron data from alpha-chitin on D19 from both hydrogen and specifically deuterated samples. From these data we expect to determine a complete atomic resolution structure including the hydrogen bonding network.

Experimental Report

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Data Citation

The recommended format for citing this dataset in a research publication is in the following format:

NISHIYAMA Yoshiharu; FORSYTH Victor Trevor; ISOBE Noriyuki; LANGAN Paul; OGAWA Yu and WADA Masahisa. (2012). Neutron studies of alpha-chitin. Institut Laue-Langevin (ILL) doi:10.5291/ILL-DATA.8-01-390

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Metadata

Experiment Parameters

  • Environment temperature

    ambient
  • Experiment energy

    1.5A
  • Experiment res energy

    1%
  • Experiment res moment

    1A

Sample Parameters

  • Formula

    • polysaccharide
  • Consistence

    polycristalline
  • Mass

    200
  • Size

    50
  • Surface

    100
  • Space

    p212121