DOI > 10.5291/ILL-DATA.CRG-2762

This proposal is publicly available since 12/13/2021

Title

Investigation of Static Sequential Infiltration Synthesis into Polystyrene-block-Maltoheptaose by neutron reflectivity

Abstract

In block copolymer lithography, metal oxide is often infiltrated selectively into one block, to establish high etch selectivity between blocks. This work investigates two different infiltration methods, where Alumina is infiltrated into 12 nm pitch Polystyrene-block-Maltoheptaose. A previous data collection of multiple pulse infiltration was made at Super-ADAM, ILL in February 2020, where analysis is ongoing. The proposed data set focuses on static (single pulse) sequential infiltration synthesis, which is a less material consuming process, but an initial test still indicates infiltration of more material per cycle. The study is expected to be of use in nanofabrication of sub-10 nm features.

Experimental Report

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Data Citation

The recommended format for citing this dataset in a research publication is in the following format:

Anette Löfstrand and VOROBIEV Alexei. (2021). Investigation of Static Sequential Infiltration Synthesis into Polystyrene-block-Maltoheptaose by neutron reflectivity. Institut Laue-Langevin (ILL) doi:10.5291/ILL-DATA.CRG-2762

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Metadata

Experiment Parameters

  • Environment temperature

    RT
  • Experiment energy

    5.2 Å
  • Experiment res energy

    0.004 Å

Sample Parameters

  • Formula

    • Maltoheptaose
    • Polysyrene
    • Polystyrene-block-Maltoheptaose